Sample | Saponin | Alkaloids | Cardiac glycosides | Steroids | Tannin | Anthraquinones | Flavonoids |
---|---|---|---|---|---|---|---|
Leaves | + | + | + | + | - | - | + |
Roots | - | + | + | + | - | - | - |
Stem | - | + | + | + | + | - | - |
Compounds (source)* | Molecular weight | Retention time | Retention index | |
---|---|---|---|---|
1. | n-Hexadecanoic acid (S, L) | 256 | 25.43 | 1968 |
2. | 7-Hexadecenoic acid (S) | 268 | 27.24 | 1886 |
3. | 9-Hexadecenoic acid (S, L, R) | 254 | 27.76 | 1976 |
4. | Octadecanoic acid (S, L) | 284 | 28.06 | 2167 |
5. | 1-Butanamine (S) | 155 | 29.58 | 1103 |
6. | 1,9-Nonanediol (S, R) | 160 | 31.63 | 1401 |
7. | Hexadecanoic acid (S, L, R) | 330 | 31.94 | 2498 |
8. | 3-Bromooctane (S) | 192 | 32.37 | 1049 |
9. | 1,3-Tetradecenal (S) | 210 | 33.88 | 1591 |
10. | 2-Quinolinecarboxylic acid (S) | 421 | 38.31 | 2310 |
11. | N,N’-Bis (p-Methoxybenxylidine) benzidine (S, L, R) | 420 | 38.50 | 3749 |
12. | N-Formylkorupensamin b (S, L) | 407 | 39.28 | 3792 |
13. | 4-Acetoxy-6′,7-dimethyl-5′,8′-dimethoxy-1,2′-binaphthalene-1′,4′,5,8-tetrone (S) | 460 | 41.97 | 3926 |
14. | 4-Pentadecyne (S) | 242 | 42.69 | 1755 |
15. | Stigmasterol,22,23-dihydro- (S) | 414 | 44.14 | 2731 |
16. | Bicyclo[3.1.0]hexan-3-ol (S) | 154 | 45.35 | 1079 |
17. | (Z)6,(Z)9-Pentadecadien-1-ol (L) | 224 | 31.56 | 1771 |
18. | 13-Oxabicyclo[10.1.0]tridecane (L) | 182 | 33.88 | 1450 |
19. | 7-Tetradecenal (L) | 210 | 31.63 | 1609 |
20. | Squalene (L, R) | 410 | 35.58 | 2914 |
21. | Silane (L) | 442 | 35.78 | 2647 |
22. | Beta-Tocopherol (L, R) | 416 | 38.30 | 3036 |
23. | 1H,3H-Furo[3,4-c]furan (L, R) | 446 | 39.28 | 3243 |
24. | Vitamin E (dl-alpha-Tocopherol) (L, R) | 430 | 39.96 | 3149 |
25. | Gamma-Sitosterol (L) | 414 | 44.14 | 2731 |
26. | 3,6-Octadien-1-ol,3,7-dimethyl-(Z)- (L) | 154 | 45.37 | 1228 |
27. | Cyclopentanol,3-methyl-2-(2-pentenyl)- (L) | 168 | 46.09 | 1315 |
28. | Decane, 1-chloro- Decyl Chloride (R) | 176 | 44.13 | 1240 |
29. | 3-Octadecyne (R) | 250 | 45.34 | 1828 |
30. | 2-Isopropyl-5-methylcyclohexymethanol (R) | 170 | 42.68 | 1280 |
31. | 9-Octadecenoic acid (R) | 296 | 27.24 | 2085 |
32. | 1-Fluorononane (R) | 146 | 31.93 | 889 |
33. | 3,8-Dibenzoyl-1-nitro-3,6,8-triazabicyclo[4.3.1]decane (R) | 394 | 32.83 | 3353 |
34. | Oxalic acid (R) | 368 | 28.68 | 2606 |
35. | 2,2,3,3,4,4,-Hexamethyltetrahydrofuran (R) | 156 | 29.58 | 992 |
1 | 2 | 3 | 4 | 5 | 6 | 7 | 8 | 9 | 10 | 11 | 12 | |
---|---|---|---|---|---|---|---|---|---|---|---|---|
Mg/ml | ASF NIG/99 (+) | Acetone (C) | Hexane(C) | DCM (C) | Chloroform (C) | Methanol (C) | Hexane (F) | Methanol (F) | Ethyl acetate (F) | Chloroform (F) | Blank | Placebo (−) |
1 | +++ | - | + | - | ++ | - | - | - | - | + | - | |
0.5 | +++ | - | ++ | - | ++ | - | - | - | - | + | - | |
0.25 | +++ | - | ++ | - | ++ | - | - | - | - | ++ | - | |
0.125 | +++ | - | +++ | - | +++ | - | - | - | + | ++ | - | |
0.0625 | +++ | - | +++ | + | +++ | - | - | + | + | +++ | - | |
0.03125 | +++ | + | +++ | ++ | +++ | ++ | + | ++ | ++ | +++ | - | |
0.015625 | +++ | ++ | +++ | ++ | +++ | ++ | ++ | ++ | ++ | +++ | - | |
0.0078125 | +++ | +++ | +++ | +++ | +++ | +++ | +++ | +++ | +++ | +++ | - |
1 | 2 | 3 | 4 | 5 | 6 | 7 | 8 | 9 | 10 | 11 | 12 | |
---|---|---|---|---|---|---|---|---|---|---|---|---|
mg/ml | ASF NIG/99 (+) | Acetone (C) | Hexane(C) | DCM (C) | Chloroform (C) | Methanol (C) | Hexane (F) | Methanol (F) | Ethyl acetate (F) | Chloroform (F) | Blank | Placebo (−) |
1 | + | * | * | * | * | * | * | * | * | * | - | |
0.5 | + | * | * | * | * | * | * | * | * | * | - | |
0.25 | + | * | * | * | * | * | * | * | * | * | - | |
0.125 | + | * | * | * | * | * | * | * | * | * | - | |
0.0625 | + | * | * | * | * | * | * | * | * | * | - | |
0.03125 | + | * | * | * | * | * | * | * | * | * | - | |
0.015625 | + | * | * | * | * | * | * | * | * | * | - | |
0.0078125 | + | * | * | * | * | * | * | * | * | * | - |
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